A, Elsagh and M, Tahernejad,
“Morphology and size of Silica Nano particles synthesized with different acids and optimize the synthesis conditions in the environment with pH less than 2”, J of Nanomaterials., Vol. 3 (7), pp. 50-57, 2012.
H, Shibata. Y, Chiba. T, Kineri. M, Matsumoto and K, Nishioa, “The effect of heat treatment on the interplanar spacing of the mesostructure during the synthesis of mesoporous MCM-41 silica Colloids and Surfaces A: Physicochem”, Eng. Aspects, 358, pp.1-5, 2010.
-51 D, Zhang. X, Wang. Z, Qiao. D, Tang. Y,
Liu and Q, Huo,”Synthesis and
Characterization of Novel Lanthanide (III) Complexes-Functionalized Mesoporous Silica
Nanoparticles as Fluorescent Nanomaterials”, J. Phys. Chem., Vol. 114, pp. 12505-12510, 2010.
منابع
D, Edimar. R, Cláudio. N, Osvaldo. A, Serra and A.G.S, Prado, “Antenna Effect in Highly Luminescent Eu3+ Anchored in Hexagonal
Mesoporous Silica”, Chem. Mater., Vol. 19 (22), pp. 5437-5442, 2007.
S.G, Weber and H, Marsmann, “From Nanosize Silica Spheres to Three-Dimensional Colloidal Crystals Siegmund Greulich-Weber and Heinrich Marsmann in Ordered Porous Nanostructures and Applications”, Nanoscale Science and Technology Series, Kluwer Academic Plenum Publisher, New York, ed. R. Wehrspohn, pp. 350-351, 2005.
L, Zhang. D, Pornpattananangkul. C.M.J, Hu and C.M, Huang, “Development of Nanoparticles for Antimicrobial Drug Delivery”, Current Medicinal Chemistry., Vol. 17, pp. 585-594, 2010.
J, António. A, Almeida and B.E, Souto, “Solid lipid nanoparticles as a drug delivery system for peptides and proteins”, Advanced Drug Delivery Reviews., Vol. 59, pp. 478490, 2007.
Y, Qiao. H, Chen. Y, Lin. Z, Cheng and J,
Huang, “Photoluminescent Lanthanide-Doped Silica Nanotubes: Sol-Gel Transcription from Functional Template”, J. Phys. Chem. C, Vol. 115 (15), pp. 7323-7330, 2011.
A, Pénard. T, Gacoin and J, Boilot, “Functionalized Sol-Gel Coatings for Optical Applications”, Acc. Chem. Res., Vol. 40 (9), pp. 895-902, 2007.
W, Scherer, Sol-Gel Science: The Physics and Chemistry of Sol-Gel Processing. Academic Press. ISBN 0121349705, 1990. 8- Q, He and J, Shi, “Mesoporous silica nanoparticle based nano drug delivery systems: synthesis, controlled drug release and delivery, pharmacokinetics and biocompatibility”, J. Mater. Chem., Vol. 21, p. 5845, 2011.
M.G, Kong. M, Keidar and K, Ostrikov, “Plasmas meet nanoparticles where synergies can advance the frontier of medicine”, J. Phys. D: Appl. Phys., Vol. 44, pp.174-188, 2011.
K, Kurumada and H, Nakabayashi, “Tsuyoshi Murataki and Masataka Tanigaki. Structure and formation process of silica microparticles and monolithic gels prepared by the sol-gel method”, Colloids and Surfaces
پيوستها
جدول 1- سنتز نمونه ها مطابق روش عمومي سل- ژل
استيك اسيد (ميلي ليتر) تترا اتيل اورتو سيلان
(ميلي ليتر) آب بدون يون (ميلي ليتر)
9 4/5 1/6

شكل 1- تصوير SEM از نمونه سنتز شده با روش عمومي سل- ژل.

شكل 2- تصوير TEM از نمونه هاي سنتز شده.

شكل 3- منحني هاي TGA نمونه سنتز شده.

شكل
4

طيف

XRD
شده

سنتز

نمونه

.

شكل

4

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